Synthesis on Scale Symposium: Process Chemistry in the Pharmaceutical Industry

Rutgers University Department of Chemistry & Chemical Biology, 123 Bevier Road, Piscataway, NJ, 08854 123 Bevier Road, Piscataway, United States

Presented by the Princeton ACS and Rutgers University. A series of talks will be given on January 12, 2024 from 9:30 to 3:45 pm. Speakers include Harshkumar Patel from Bristol-Myers Squibb, Kevin Campos from Merck, Chris Senanayake from TCG GreenChem, and Prof. Kendall Houk from UCLA. They will cover a range of topics from innovations in synthetic chemistry to computational elucidation of reactions. Register for the event here. Registration for undergrad and graduate students is $20, and parking is free! See the attachment and registration page for more information.

Meeting of the Princeton ACS Section:“1D Lepidocrocite Titania-based Nanomaterials, Their Diverse Morphologies and Exceptional Properties”

Frick Chemistry Laboratory, Taylor Auditorium, Princeton University

Meeting of the Princeton ACS Section Tuesday, March 12, 2024 Professor Michel. W. Barsoum Drexel University, Philadelphia, PA “1D Lepidocrocite Titania-based Nanomaterials, Their Diverse Morphologies and Exceptional Properties” Frick Chemistry Laboratory, Taylor Auditorium, Princeton University Mixer (in Atrium) 6:30 pm; Lecture 7:00 pm   Abstract: Recently, we converted 15 binary and ternary titanium carbides, nitrides, borides, phosphides, and silicides into lepidocrocite-based, one dimensional, 1D, sub-nanometer nanofilaments, NFs, ≈ 5x7 Å in cross-section by reacting them with a tetramethylammonium hydroxide, TMAH, aqueous solution at ≈ 85 °C range for tens of hours. In some cases, the conversion is 100 % precluding the need for centrifuges, filters, etc. We currently routinely make 100 g batches in a lab setting. Depending on with what and the order the reaction products are washed, the 1D NFs self-assemble into loose, spaghetti-shaped fibers, ≈ 30 nm in diameter, fully inorganic TiO2 gels, pseudo 2D or porous mesoscopic particles. In all cases, the fundamental building block is 1D lepidocrocite NFs, ≈ 3 nm long, that self-assemble into the aforementioned morphologies. At this time, we believe that our materials are the only thermodynamically stable 1D NFs in water, with important implications in photo- and chemical catalysis. The production

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